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11.
The accurate and precise determination of Li isotopic composition by MC‐ICP‐MS suffers from the poor performance of traditional column chromatography. Previously established chromatographic processes cannot completely remove Na in complex geological samples, which is currently interpreted to be a result of Na breakthrough. In this study, Na breakthrough during single‐column purification was found to differ between simply artificial Na‐containing sample solutions, where a little Na residue was found, and silicate rocks, where a large amount of breakthrough occurred. A revised two‐step column purification for Li using 0.5 and 0.3 mol l?1 HCl as eluents was designed to remove the Na. This modified method achieves high‐efficiency Li purification from Na and consequently avoiding high Na/Li ratio interference for subsequent MC‐ICP‐MS analyses. The proposed method was validated by the analysis of a series of reference materials, including Li2CO3 (IRMM‐016, ‐0.10‰), basalt (BCR‐2: 2.68‰; BHVO‐2: 4.39‰), andesite (AGV‐2: 6.46‰; RGM‐2: 2.59‰), granodiorite (GSP‐2: ?0.87‰) and seawater (CASS‐5, 30.88‰). This work reports early Na appearance prior to the elution curves in chromatography and emphasises its influence for subsequent Li isotope measurement. Based on the findings, the established two‐step method would be more secure than single‐column chemistry for Li purification. 相似文献
12.
Wang Xiangdong Hu Keyi Qie Wenkun Sheng Qingyi Chen Bo Lin Wei Yao Le Wang Qiulai Qi Yuping Chen Jitao Liao Zhuoting Song Junjun 《中国科学:地球科学(英文版)》2019,62(1):135-153
The Carboniferous period lasted about 60 Myr, from ~358.9 Ma to ~298.9 Ma. According to the International Commission on Stratigraphy, the Carboniferous System is subdivided into two subsystems, i.e., Mississippian and Pennsylvanian, including 6 series and 7 stages. The Global Stratotype Sections and Points(GSSPs) of three stages have been ratified, the Tournaisian, Visean, and Bashkirian stages. The GSSPs of the remaining four stages(i.e., the Serpukhovian, Moscovian,Kasimovian, and Gzhelian) have not been ratified so far. This paper outlines Carboniferous stratigraphic subdivision and correlation on the basis of detailed biostratigraphy mainly from South China, and summarizes the Carboniferous chronostratigraphic framework of China. High-resolution biostratigraphic study reveals 37 conodont zones, 24 foraminiferal(including fusulinid) zones, 13 ammonoid zones, 10 brachiopod zones, and 10 rugose coral zones in the Carboniferous of China. The biostratigraphic framework based on these biozones warrants the precise correlation of regional stratigraphy of China(including2 subsystems, 4 series, and 8 stages) to that of the other regions globally. Meanwhile, the Carboniferous chemo-, sequence-,cyclo-, and event-stratigraphy of China have been intensively studied and can also be correlated worldwide. Future studies on the Carboniferous in China should focus on(1) the correlation between shallow-and deep-water facies and between marine and continental facies,(2) high-resolution astronomical cyclostratigraphy, and(3) paleoenvironment and paleoclimate analysis based on geochemical proxies such as strontium and oxygen isotopes, as well as stomatal indices of fossil plants. 相似文献
13.
轨道交通周边土地开发和溢价归公有助于缓解城市财政压力,推动公交都市建设。结合国外实施溢价归公的政策和实践模式,以东莞市为例,在资料收集、政策分析、文本和案例解读的基础上,探讨了中国城市政府在规划和建设轨道交通中,以土地溢价归公反哺轨道交通融资的政策安排和实施效果。结果表明:1)溢价归公的本质是以特定方式实现正外部效应的内部化,由于土地制度和税收体系的差异,欧美地区溢价归公主要依赖多样化的土地税收体系,而中国城市的实践主要借鉴了“轨道+物业”的联合开发模式;2)东莞市溢价归公策略的形成是综合开发规划编制和审批、沿线土地控制和储备、土地发展权转移、土地增值分配等核心环节有效协调的结果;3)东莞轨道交通沿线土地开发能形成可观的财政收益,潜在土地收益占轨道资金总需求的比例超过20%,但在实施过程中仍面临较大困难。东莞市案例能为其他城市轨道交通融资、土地开发和溢价归公的政策体系编制和有效实施提供一定的参考。 相似文献
14.
15.
Earthquake simulation technologies are advancing to the stage of enabling realistic simulations of past earthquakes as well as characterizations of more extreme events, thus holding promise of yielding novel insights and data for earthquake engineering. With the goal of developing confidence in the engineering applications of simulated ground motions, this paper focuses on validation of simulations for response history analysis through comparative assessments of building performance obtained using sets of recorded and simulated motions. Simulated ground motions of past earthquakes, obtained through a larger validation study of the Southern California Earthquake Center Broadband Platform, are used for the case study. Two tall buildings, a 20‐story concrete frame and a 42‐story concrete core wall building, are analyzed under comparable sets of simulated and recorded motions at increasing levels of ground motion intensity, up to structural collapse, to check for statistically significant differences between the responses to simulated and recorded motions. Spectral shape and significant duration are explicitly considered when selecting ground motions. Considered demands include story drift ratios, floor accelerations, and collapse response. These comparisons not only yield similar results in most cases but also reveal instances where certain simulated ground motions can result in biased responses. The source of bias is traced to differences in correlations of spectral values in some of the stochastic ground motion simulations. When the differences in correlations are removed, simulated and recorded motions yield comparable results. This study highlights the utility of physics‐based simulations, and particularly the Southern California Earthquake Center Broadband Platform as a useful tool for engineering applications. 相似文献
16.
颗粒物粒径分布(Particle Size Distribution, PSD)代表了颗粒物浓度与颗粒物粒径之间的关系, 影响着海洋生态环境和水体光学特性等。文章基于2016年夏季航次调查的生物光学剖面数据, 研究了南海海盆海域PSD的分布特征。研究发现, 幂律函数可以较好地拟合南海海盆区域的PSD, 对数空间中的实测的PSD与模拟的PSD平均决定系数高达0.95。PSD斜率(ξ)的分布范围为[1.27, 7.65], 均值为3.93±0.56。南海海盆区域表层水体的ξ均值与全球大洋表层水体的ξ均值相近, 但高于海湾等表层水体的ξ均值。ξ能较好地表征颗粒物平均粒径DA的大小, 两者存在明显负相关关系, 即ξ值越高, DA越小; 反之, DA越大。通过分析T1断面的生物光学剖面数据及总体平均的PSD剖面数据, 发现PSD剖面分布特征如下: 1)表层水体的ξ值相对较高, 且DA值相对较低, 推测可能是由于微微型藻类为主导颗粒物所致; 2) ξ值极小值层出现在次表层叶绿素浓度极大值层(Subsurface Chlorophyll Maximum Layer, SCML)中, 并伴随DA极大值层的出现, 其原因可能是SCML中的大粒径浮游植物占比显著增加; 3)弱光层中的ξ值较SCML中的高, 但略低于表层的ξ值, 而DA则位于表层与SCML的DA之间, 这可能与浮游植物及其碎屑的絮凝、分解、沉降等过程相关。PSD特征影响着海水的固有光学特性, 分析发现: 由于SCML中的叶绿素浓度增加, 颗粒物散射系数(bp(532))和颗粒物后向散射系数(bbp(532))也相应呈现显著增加的趋势。弱光层中的平均bp(532)与平均bbp(532)最小。ξ与颗粒物衰减光谱斜率之间呈高分散性, Boss 等(2001b) 的模型适合用于粗略估算区域性的ξ分布范围及均值。 相似文献
17.
参对光照变化非常敏感,研究刺参对光照的分子响应非常重要。本研究应用RNA测序获取了刺参暴露于强光(“强光”)、正常光照(“对照”)和完全黑暗(“黑暗”)环境下体壁的基因表达谱情况,通过“对照”与“黑暗”,“对照”与“强光”和“黑暗”与“强光”的比较,在|log2 ratio|≥1和FDR≤0.001的标准下分别发现了1161、113和1705个差异表达基因(DEGs)。基因本体分析表明,“cellular process”和“binding”在“生物过程”和“分子功能”类别中的DEGs富集最多,而“cell”和“cell part”在“细胞组分”类别中的DEGs富集最多。将DEGs与Kyoto Encyclopedia基因和基因组数据库上的于214、41和229条通路进行比对,发现了51、2和57条通路分别显著富集。本研究发现的光特异性DEGs可作为深入研究刺参对光照变化的生化适应机制的重要目标基因。 相似文献
18.
19.
随着海洋开发活动的不断加剧,各海洋开发类型综合效益的评估与分析对维持海洋社会经济与海洋生态环境的可持续发展具有重大意义,不同海洋开发活动带来不同的社会、经济效益,也产生了海洋资源的损耗,影响了海洋环境和海洋生态服务功能。根据江苏省海洋资源开发活动特点,筛选出江苏海岸带资源开发中常见的4种典型的开发利用类型,选取了能够突出反映海洋开发活动综合效益的经济效益指标、社会效益指标、资源损耗指标、环境成本指标构建海洋开发类型综合效益评估体系。基于层次分析法与熵权法组合权重,运用综合效益指数评价模型分别计算了单一指标效益值、准则层效益值、各研究案例效益值、各用海类型效益值并对以上研究数据之间的相互关系进行了深入分析,探求各用海类型综合效益评估值的关键影响因素。通过实证研究发现4种海洋开发类型的综合效益评估值均介于0.4~0.6之间,处于一般的综合效益状态,综合效益从高到底依次排序:临港工业用海类型为0.551 3、海上风电用海类型为0.492 4、排污倾倒用海类型为0.441、围海养殖用海类型为0.434 3。海洋开发类型综合效益的评估对及时调整海洋开发对策,缓和海洋开发与海洋生态环境的矛盾具有积极意义。 相似文献
20.
Variation in soil saturated hydraulic conductivity along the hillslope of collapsing granite gullies 总被引:2,自引:0,他引:2
Saturated hydraulic conductivity (Ks) affects the soil hydrological process and is influenced by many factors that exhibit strong spatial variations. To accurately measure Ks and its scale, spatial variability and relationship with collapsing gullies, we analysed four double-ring infiltrometer diameters in three soil layers during in situ experiments designed to measure Ks in two typical collapsing gullies (three slope sites) in Tongcheng County of China. The results showed that Ks increased with increasing inner ring diameter, but no significant difference existed between inner diameters of 30 and 40 cm. The Ks in red soil layers was higher than that in sandy soil layers, the transition layers had the lowest values. Ks also varied with slope position, gradually decreasing with distance from the gully head. The suggestion is that the spatial variation in Ks is affected not only by the intrinsic soil properties but also by the interaction with the collapsing gully. 相似文献